Remember : Tips Precautions for the use of alumina corundum tube:1. The temperature difference is too large. When using, put the heat insulation plug (two on each side) in the corundum tube, the position is between the hot zone and the cold zone.
2. The middle of the tube is relatively soft at such a high temperature, so the tube is easier to deform and break. It is recommended to add brackets on both sides of the pipe. The brackets can reduce deformation and breakage.
3. The newly-purchased tube needs to be bake several times at different temperatures before using the corundum tube newly bought here, generally bake several times. It is generally kept at 200 C-1000°C for 1 hour.
4. It is recommended that the heating rate should not be too fast, and should not exceed the fastest heating rate of 140°C/h, and the fastest limit speed of 10°C/min. Special attention should be paid to cooling! The name of the best heating rate should not be higher than 10°C/min, cooling down The rate should be less than 10°C/min.
5. In addition to the above bracket problem; also, the samples burned in the tube furnace, especially the samples to be burned to about 1300 ℃, preferably have less water content (water content refers to adsorbed water, crystal water, etc., Water that may be generated during the heating process) It is recommended that your sample be pre-burned and then put into the tube furnace. It is best not to take or add samples at high temperatures, which may damage the furnace tube of the corundum.
6. Do not touch the corundum furnace tube strongly, do not keep the temperature at 300°℃-900℃, do not touch the high temperature furnace tube with low temperature objects. 7. Below 500°℃≤5℃/min; 500-800℃≤10℃/min; 800-1000℃≤5℃/min; 1000-1400℃≤3℃/min; 1400-1600°C≤2℃/min . The recommended heating rate is used.